COMPARATIVE EVALUATION OF THE ANTIOXIDANT ACTIVITY OF SPICE EXTRACTS AND MODEL ANTIOXIDANTS IN A LIPID SYSTEM
DOI:
https://doi.org/10.31073/foodresources2026-26-07Keywords:
antioxidants, spice extracts, lipid oxidation, sunflower oil, marjoram, marinades, oxygen uptaleAbstract
Subject. The article is devoted to the study of the antioxidant activity of spice extracts in a lipid system and the assessment of their potential as natural inhibitors of oxidation in food products. Purpose. To evaluate the effectiveness of spice extracts (marjoram, allspice, clove, cumin, and rosemary) as natural antioxidants in a model sunflower oil system, to compare their activity with model antioxidants, and to determine their potential application in food technologies, particularly in marinades. Methods. The antioxidant activity was determined using an experimental method based on the kinetics of oxygen uptake. Sunflower oil samples containing spice extracts and model antioxidants were subjected to vacuum treatment followed by oxygen saturation. The experiments were carried out at 70 °C. Azobisisobutyronitrile was used as an oxidation initiator. The obtained data were processed using analytical methods and logical generalization. Results. All studied spice extracts exhibited antioxidant activity, which depended on their nature and concentration. An increase in concentration up to 1% resulted in a significant reduction in the oxidation rate. The most pronounced antioxidant effect under the experimental conditions was observed for marjoram extract (1%), which showed the lowest oxygen uptake. Clove and allspice extracts also demonstrated high efficiency but were less effective than marjoram. It was shown that natural extracts can approach the effectiveness of model antioxidants such as α-tocopherol and ascorbyl palmitate. Application of results. The obtained results can be used for the development of food formulations with improved oxidative stability, particularly sauces and oil-based marinades, as well as for reducing the use of synthetic antioxidants.
Downloads
References
1. Hennebelle, M., Villeneuve, P., Durand, E., Lecomte, J., van Duynhoven, J., Meynier, A., Yesiltas, B., Jacobsen, C., & Berton-Carabin, C. (2024). Lipid oxidation in emulsions: New insights from the past two decades. Progress in lipid research, 94, 101275. https://doi.org/10.1016/j.plipres.2024.101275.
2. Laguerre, M., Lecomte, J., & Villeneuve, P. (2007). Evaluation of the ability of antioxidants to counteract lipid oxidation: existing methods, new trends and challenges. Progress in lipid research, 46(5), 244–282. https://doi.org/10.1016/j.plipres.2007.05.002.
3. Brewer, M.S. (2011), Natural Antioxidants: Sources, Compounds, Mechanisms of Action, and Potential Applications. Comprehensive Reviews in Food Science and Food Safety, 10: 221–247. https://doi.org/10.1111/j.1541-4337.2011.00156.x.
4. Rathod, N. B., Kulawik, P., Özoğul, F., Regenstein, J. M., & Ozogul, Y. (2021). Biological activity of plant-based carvacrol and thymol and their impact on human health and food quality. Trends in Food Science & Technology, Article 116. https://doi.org/10.1016/j.tifs.2021.08.023.
5. Miguel, M. G. (2010). Antioxidant and Anti-Inflammatory Activities of Essential Oils: A Short Review. Molecules, 15(12), 9252–9287. https://doi.org/10.3390/molecules15129252.
6. Andrade, B. F., Ferreira, V. R. F., Cardoso, G. P., Andrade, M. P. D., Ramos, A. L. S., Cardoso, M. G., & Ramos, E. M. (2023). Allspice (Pimenta Dioica Lindl) leaves essential oil as a potential antioxidant and antimicrobial source for use in mechanically deboned poultry meat. Brazilian Journal of Food Technology, 26, e2022125. https://doi.org/10.1590/1981-6723.12522.
7. Gülçin İ. (2011). Antioxidant activity of eugenol: a structure-activity relationship study. Journal of medicinal food, 14(9), 975–985. https://doi.org/10.1089/jmf.2010.0197.
8. Chaieb, K., Hajlaoui, H., Zmantar, T., Kahla-Nakbi, A. B., Rouabhia, M., Mahdouani, K., & Bakhrouf, A. (2007). The chemical composition and biological activity of clove essential oil, Eugenia caryophyllata (Syzygium aromaticum L. Myrtaceae): A short review. Phytotherapy Research, 21(6), 501–506. https://doi.org/10.1002/ptr.2124.
9. Shan, B., Cai, Y. Z., Sun, M., & Corke, H. (2005). Antioxidant capacity of 26 spice extracts and characterization of their phenolic constituents. Journal of Agricultural and Food Chemistry, 53(20), 7749–7759. https://doi.org/10.1021/jf051513y.
10. Ramos, M., Beltrán, A., Peltzer, M.A., Valente, A.J., & Garrigós, M.C. (2014). Release and antioxidant activity of carvacrol and thymol from polypropylene active packaging films. Lwt - Food Science and Technology, 58, 470–477. https://doi.org/10.1016/j.lwt.2014.04.019.
11. Tasan, M. (2004). Total and individual tocopherol contents of sunflower oil at different steps of refining. European Food Research and Technology. https://doi.org/10.1007/S00217-004-1045-8.
12. Laguerre, M., Lecomte, J., & Villeneuve, P. (2007). Evaluation of the ability of antioxidants to counteract lipid oxidation: existing methods, new trends and challenges. Progress in lipid research, 46(5), 244–282. https://doi.org/10.1016/j.plipres.2007.05.002.
13. Nagao, A., & Yamazaki, M. (1981). Oxygen absorption method for assessing oxidative stability of fats and oils. Journal of Japan Oil Chemists' Society, 30(11), 778–780. https://doi.org/10.5650/jos1956.30.778.
14. Amorati, R., Baschieri, A., & Valgimigli, L. (2017). Measuring antioxidant activity in bioorganic samples by the differential oxygen uptake apparatus: Recent advances. Journal of Chemistry, 2017, Article 6369358. https://doi.org/10.1155/2017/6369358.
Downloads
Published
How to Cite
Issue
Section
License
Copyright (c) 2026 В. В. Ляпунов, І. М. Демидов

This work is licensed under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International License.
Licensing and Copyright
The collection provides immediate open access, ensuring that the content is freely available to the global community, facilitating a broader exchange of knowledge in accordance with the principles of open science.
By submitting an article to the editors of the collection, authors confirm that the manuscript has not been submitted to other publications and grant the journal the right of first publication in accordance with the terms of the Copyright Transfer Agreement.
Copyright. Authors retain full copyright to their articles without restriction and simultaneously grant the journal a non-exclusive license for publication, distribution, and indexing.
Licensing. The collection publishes articles under a Creative Commons Attribution-NonCommercial-NoDerivatives 4.0 International (CC BY-NC-ND 4.0) license.
https://creativecommons.org/licenses/by-nc-nd/4.0/deed.uk
This license permits:
- copying and distributing the material in any medium or format;
- use of the material for educational and research purposes.
- Subject to the following conditions:
- attribution of the author, source, and license link;
- noncommercial use;
- no distribution of modified material (no derivatives).
First Publication Rights. Authors grant the collection “Food Resources” first publication rights, these allowing the collection to distribute the scientific material with attribution of authorship and the original publication in the collection.
Self-Archiving. Authors may upload any version of their articles (preprint, postprint, or published version) to institutional, disciplinary, or personal repositories without embargo, provided they indicate that the article was published in the collection "Food Resources" and include the CC BY-NC-ND license.
ISSN
ISSN 




