PHYSICAL AND MECHANICAL METHODS IN THE PRODUCTION OF PECTIN-CONTAINING PRODUCTS FROM PLANT RAW MATERIALS

Authors

DOI:

https://doi.org/10.31073/foodresources2025-25-16

Keywords:

pectin, discrete-impulse energy input method, rotor-pulsation apparatus, cavitation, plant raw materials, hydrolysis, extraction, radioprotective properties

Abstract

Subject. Heat and mass transfer processes and physico-mechanical methods for processing plant raw materials to obtain pectin-containing products. Purpose. To investigate the efficiency of pectin extraction from plant raw materials using hydrodynamic treatment with rotor-pulsation apparatuses and the discrete-pulse energy input (DРEI) method, as well as to assess the impact of processing parameters on the quality and functional properties of the final product. Methods. Plant raw materials (apple pomace, sugar beet pulp, and carrots) were pretreated and then processed in a closed-loop circulation system equipped with a rotor-pulsation apparatus implementing the discrete-pulse energy input method. The treatment was carried out under variable hydrodynamic loading conditions, generating localized high-pressure impulse zones. Process parameters (duration, intensity, and recirculation rate) were varied to achieve optimal hydrolysis depth of protopectin and extraction of water-soluble pectin. Results. It was established that the application of the discrete-pulse energy input method and rotor-pulsation apparatus intensifies mass transfer processes, reduces hydrolysis duration by 30–40%, lowers processing temperature to 45–50 °C, and ensures a high pectin yield without loss of its functional properties. It was demonstrated that impulse action promotes the destruction of plant cell walls, preserves the native structure of the cellulose matrix, and improves the organoleptic characteristics of the final product. Scope of the results. The research findings can be used to develop industrial technologies for producing pectin concentrates and functional food products with radioprotective properties, as well as for upgrading equipment in the food and pharmaceutical industries.

Downloads

Download data is not yet available.

References

Evaluation of the use of pectin of children living in regions contaminated by caesium. Report. 2005. https://en.irsn.fr/sites/en/files/2023-10/IRSN_Report-DRPH-2005-008_Pectin.pdf (date of access: 15.10.2025).

Wang, R., Liang, R., Dai, T., Chen, J., Shuai, X., Liu, C. (2019). Pectin-based adsorbents for heavy metal ions: A review. Trends in food science & technology, 91, 319–329. https://doi.org/10.1016/j.tifs.2019.07.033.

Nesterenko, V., Nesterenko, A., Babenko, V., Yerkovich, T., Babenko, I. (2004). Reducing the 137Cs-load in the organism of “Chernobyl” children with apple-pectin. Swiss Med Wееkly, 10; 134(1-2):24-7, 24–28. https://doi.org/10.4414/smw.2004.10223.

Pectin market size, share, trends and forecast by raw material, end use, and region, 2025-2033. (2024). https://www.imarcgroup.com/pectin-technical-material-market-report.

Yapo, B., Robert, C., Etienne, I., Wathelet, B., Paquot, M. (2007). Effect of extraction conditions on the yield, purity and surface properties of sugar beet pulp pectin extracts. Food Chemistry, 100(4), 1356–1364. https://doi.org/10.1016/j.foodchem.2005.12.012.

Chen, H., Fu, X., Luo, Z. (2015). Properties and extraction of pectin-enriched materials from sugar beet pulp by ultrasonic-assisted treatment combined with subcritical water. Food Chemistry, 168 (1), 302–310. https://doi.org/10.1016/j.foodchem.2014.07.078.

Peighambardoust, S., Jafarzadeh-Moghaddam, M., Pateiro, M., Lorenzo, J., Domínguez, R. (2021). Physicochemical, thermal and rheological properties of pectin extracted from sugar beet pulp using subcritical water extraction process. Molecules, 26 (5), 1413. https://doi.org/10.3390/molecules26051413.

Martyniuk, A., Pastukh, H. (2019). Current trends in sugar production waste disposal. Environmental sciences, 2(25), 187–190. https://doi.org/10.32846/2306-9716-2019-2-25-31. [in Ukrainian].

Litvynenko, O. A., Nekoz, O. I., Horbach, O. M. (2011). Sposib vyrobnytstva pektinvmisnykh produktiv z roslynnoi syrovyny [Method for producing pectin-containing products from plant raw materials]: Ukrainian Patent № 65942. Natsionalnyi universytet kharchovykh tekhnolohii [National University of Food Technologies]. Filed March 9, 2011. Published December 26, 2011, Bulletin No. 24. [in Ukrainian].

Luhovskyi, O. F., Bernyk, I. M. (2008). Vykorystannia fizychnykh poliv dlia hidrolizu-ekstraktsii protopektynu roslynnoi syrovyny [Use of physical fields for hydrolysis-extraction of protopectin from plant raw materials]. Vibratsii v tekhnitsi ta tekhnolohiiakh [Vibrations in engineering and technology], 3 (52), 92–100. [in Ukrainian].

Bernyk, I. M. (2009). Vstanovlennia optymalnykh parametriv tekhnolohichnoho protsesu vyluchennia pektinu z yabluchnykh vychavok v ultrazvukovomu poli [Determination of optimal parameters of the technological process of pectin extraction from apple pomace in an ultrasonic field]. Visnyk Natsionalʹnoho tekhnichnoho universytetu “Kharkivskyi politekhnichnyi instytut”. Tematychnyi vypusk “Khimia, khimichna tekhnolohiia ta ekolohiia” [Bulletin of the National Technical University “Kharkiv Polytechnic Institute”. Thematic issue “Chemistry, Chemical Technology and Ecology”], 45, 21–27. [in Ukrainian].

Bernyk, I. M., Luhovskyi, O. F., Krapyvnytska, I. O. (2010). Osoblyvosti vyluchennia pektinu v ultrazvukovomu kavitatsiinomu poli ta yoho vlastyvosti [Features of pectin extraction in an ultrasonic cavitation field and its properties]. Naukovi pratsi Natsionalʹnoho universytetu kharchovykh tekhnolohii [Scientific Works of the National University of Food Technologies], (32), 59–63. [in Ukrainian].

Luhovskyi, O. F., Bernyk, I. M. (2010). Fizychna modelʹ ultrazvukovoho kavitatsiinoho vyluchennia pektinu z vtorynnoi roslynnoi syrovyny [Physical model of ultrasonic cavitation extraction of pectin from secondary plant raw materials]. Visnyk Natsionalʹnoho tekhnichnoho universytetu Ukrainy “Kyivskyi politekhnichnyi instytut”, seriia “Khimichna inzheneriia, ekolohiia ta resursozberezhennia” [Bulletin of the National Technical University of Ukraine“Kyiv Polytechnic Institute”, Series “Chemical Engineering, Ecology and Resource Saving”], 1 (5), 25–30. [in Ukrainian].

Lytvynenko, O. A., Nekoz, O. I., Nemyrovych, P.M., Kondrat, Z. (1999). Kavitatsiini prystroi v kharchovii, pererobnii ta farmatsevtychnii promyslovosti [Cavitation devices in food, processing and pharmaceutical industries]. Kyiv: RVC UDUKhT. 87 р. ISBN 966-612-004-6. [in Ukrainian].

Luhovskyi, O. F., Bernyk, I. M. (2001). Vyrobnytstvo pektynovoho kontsentratu z vykorystanniam ultrazvukovykh kavitatsiinykh tekhnolohii [Production of pectin concentrate using ultrasonic cavitation technologies]. Zbirnyk naukovykh prats Vinnytskoho natsionalʹnoho ahrarnoho universytetu [Collected Scientific Works of Vinnytsia National Agrarian University], 9, 159–163. [in Ukrainian].

Dolinskiy, A. A. (2015). Pryntsyp dyskretno-impul'snoho vvodu enerhiyi ta yoho vykorystannya u tekhnolohichnykh protsesakh [The principle of discrete-pulse energy input and its use in technological processes]. Mikro- i nanourovnevyye protsessy v tekhnologiyakh DIVE: Tematicheskiy sbornik statey; Institut tekhnicheskoy teplofiziki NAN Ukrainy. [Micro- and nanoscale processes in DPEI technologies: Thematic collection of articles] – К. Akademperiodika. 464 р. [in Ukrainian].

Obodovych, O. M., Khomenko, V. O., Sydorenko, V. V., Stepanova, O. Ye. (2024). Dyskretno-impulʹsnyi vvod enerhii (DIVE) ta yoho realizatsiia shliakhom zastosuvannia rotorno-pulsatsiinykh aparativ [Discrete-pulse energy input (DPEI) and its implementation using rotor-pulsation devices]. Teplofizyka ta teploenerhetyka [Thermophysics and Thermal Power Engineering], 46(1), 29–38. https://doi.org/10.31472/ttpe.1.2024.4.

Obodovych, A. N., Khibina, M. A., Boryak, L. A., Obodovych, A. A., Teslia, A. I. (2006). Intensifikatsiia proizvodstva hliukozo-fruktoznykh syropov za schet mekhanokhimicheskoi destruktsii [Intensification of glucose-fructose syrup production through mechanochemical destruction]. Promyshlennaia teplotekhnika [Industrial Heat Engineering], 28(3), 44–49. [in russian].

Obodovych, A. N., Lymar, A. Yu. (2013). Diskretno-impulʹsnyi vvod enerhii (DIVE) – intensyfikuiushchyi metod hydroliza vysokomolekuliarnykh soedinenii [Discrete-pulse energy input (DPEI) – an intensifying method of hydrolysis of high-molecular compounds]. Promyshlennaia teplotekhnika [Industrial Heat Engineering], 35(6), 23–30. [in russian].

Dolinskiy, A. A., Ivanitskiy, G. K. (2008). Teplomassoobmen i gidrodinamika v paro-zhidkostnykh dispersnykh sredakh. Teplofizicheskie osnovy diskretno-impulʹsnogo vvoda energii [Heat and mass transfer and hydrodynamics in vapor-liquid dispersed media. Thermophysical foundations of discrete-impulse energy input]. Kyiv: Naukova Dumka, 304 р. [in russian].

Chemat, F., Khan, M. K. (2011). Applications of ultrasound in food technology: Processing, preservation and extraction. Ultrason. Sonochem, 18, 813–835. https://doi.org/10.1016/j.ultsonch.2010.11.023.

Lijun Wang, Curtis L.Weller. (2006). Recent advances in extraction of nutraceuticals from plants. Trends in Food Science & Technology. 17, 300–312. https://doi.org/10.1016/j.tifs.2005.12.004.

Roctagno, M. and Prado, J. (Ed.). (2013). Natural product extraction: Principles and applications. Royal Society of Chemistry, Cambridge, UK. 516 р. https://doi.org/10.1039/9781849737579.

Sensoy, I., Sastry, S. K. (2004). Extraction using moderate electric fields. Journal of Food Science, 69(1), 7-13. https://doi.org/10.1111/j.1365-2621.2004.tb17861.x.

Roohinejad, Sh., Koubaa, M., Greiner, R., Orlien, V., Lebovka, N. (2016). Negative pressure cavitation extraction: A novel method for extraction of food bioactive compounds from plant materials. Trends in Food Science & Technology. 52, 98–108. https://doi.org/10.1016/j.tifs.2016.04.008.

Parag, R., Gogate, P. R. (2011). Hydrodynamic cavitation for food and water processing. Food and Bioprocess Technology, 4(6), 996–1011. https://doi.org/10.1007/s11947-010-0418-1.

Shirsath, S. R., Sonawane, S. H., Gogate, P. R. (2012). Intensification of extraction of natural products using ultrasonic irradiations: A review of current status. Chemical Engineering and Processing: Process Intensification, 53, 10–23. https://doi.org/10.1016/j.cep.2012.01.003.

Published

2025-12-22

How to Cite

Obodovych, O., Husiatynska, N., Stepanova, O., Sheiko, T., Rezakova, T., & Chernyavsky, K. (2025). PHYSICAL AND MECHANICAL METHODS IN THE PRODUCTION OF PECTIN-CONTAINING PRODUCTS FROM PLANT RAW MATERIALS. FOOD RESOURCES, 13(25), 141–153. https://doi.org/10.31073/foodresources2025-25-16

Issue

Section

Технічні науки